1W7R
Feglymycin P64 crystal form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-05-15 |
| Detector | MARRESEARCH |
| Spacegroup name | P 64 |
| Unit cell lengths | 60.302, 60.302, 83.748 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 28.400 - 1.400 |
| R-factor | 0.1739 |
| R-free | 0.21970 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1w7q |
| RMSD bond length | 0.017 |
| RMSD bond angle | 0.037 |
| Data reduction software | HKL-2000 |
| Data scaling software | SADABS |
| Phasing software | EPMR |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.370 | 1.500 |
| High resolution limit [Å] | 1.400 | 1.400 |
| Rmerge | 0.060 | 0.670 |
| Number of reflections | 34149 | |
| <I/σ(I)> | 21.5 | 3.49 |
| Completeness [%] | 99.8 | 99.1 |
| Redundancy | 14.17 | 10.95 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | 0.25 M NA3CIT/H3CIT PH=6.5 30% ISOPROPANOL, pH 6.50 |
