1W7Q
Feglymycin P65 crystal form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | MACSCIENCE M06XCE |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-10-10 |
| Detector | BRUKER-NONIUS |
| Spacegroup name | P 65 |
| Unit cell lengths | 83.544, 83.544, 35.734 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 72.350 - 1.100 |
| R-factor | 0.1689 |
| R-free | 0.19500 |
| Structure solution method | DIRECT METHODS |
| RMSD bond length | 0.022 |
| RMSD bond angle | 0.045 |
| Data reduction software | SAINT |
| Data scaling software | SADABS |
| Phasing software | SHELXD |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 72.350 | 1.200 |
| High resolution limit [Å] | 1.100 | 1.100 |
| Rmerge | 0.040 | 0.450 |
| Number of reflections | 57985 | |
| <I/σ(I)> | 25.31 | 3.06 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 9.97 | 4.64 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.4 | 0.1 M TRIS/TRISHCL PH=8.4, 4% PEG8000, pH 8.40 |
