1W5J
AN ANTI-PARALLEL FOUR HELIX BUNDLE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 93 |
Collection date | 2003-03-19 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 33.691, 37.192, 103.991 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.600 - 2.200 |
R-factor | 0.231 |
Rwork | 0.228 |
R-free | 0.28500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.038 |
RMSD bond angle | 2.349 |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | CrystalClear ((MSC/RIGAKU)) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.000 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.070 | 0.160 |
Number of reflections | 7116 | |
<I/σ(I)> | 10.7 | 10.7 |
Completeness [%] | 99.3 | 99.3 |
Redundancy | 4.15 | 3.75 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | HANGING DROP, 1 UL OF 10 MG/ML PEPTIDE IN WATER TO 1UL OF 0.07M TRI-SODIUM CITRATE DIHYDRATE PH 5.6 0.7M AMMONIUM DIHYDROGEN PHOSPHATE %30 V/V GLYCEROL, HAMPTON CRYSTAL SCREEN CRYO NUMBER 11 |