1W4S
Crystal structure of the proximal BAH domain of polybromo
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-09-18 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 39.598, 57.712, 70.377 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.550 |
R-factor | 0.201 |
Rwork | 0.199 |
R-free | 0.23000 |
Structure solution method | MAD |
RMSD bond length | 0.021 |
RMSD bond angle | 1.849 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.630 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.070 | 0.260 |
Number of reflections | 23961 | |
<I/σ(I)> | 17.9 | 4.7 |
Completeness [%] | 99.4 | 100 |
Redundancy | 4.7 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 0.1M TRIS.HCL PH 8.0 0.6 TO 1.6M AMMONIUM SULPHATE 20% (W/V) SUCROSE |