1W40
T. celer L30e K9A variant
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 23.215, 54.164, 34.157 |
| Unit cell angles | 90.00, 109.79, 90.00 |
Refinement procedure
| Resolution | 32.110 - 2.030 |
| R-factor | 0.207 |
| Rwork | 0.206 |
| R-free | 0.24100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1h7m |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.110 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 17.000 | 2.140 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.050 | 0.120 |
| Number of reflections | 4994 | |
| <I/σ(I)> | 23.3 | 13.9 |
| Completeness [%] | 95.5 | 89.6 |
| Redundancy | 3.7 | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | pH 7.50 |
