1W39
Crystal structure of an artificial top component of turnip yellow mosaic virus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-02-15 |
| Detector | ADSC QUANTUM 210 |
| Spacegroup name | F 41 3 2 |
| Unit cell lengths | 688.457, 688.457, 688.457 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.000 - 3.750 |
| R-factor | 0.2453 |
| Rwork | 0.245 |
| R-free | 0.25080 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1auy |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.484 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | CNS (0.9) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.000 | 3.880 |
| High resolution limit [Å] | 3.750 | 3.750 |
| Rmerge | 0.200 | 0.600 |
| Number of reflections | 140727 | |
| <I/σ(I)> | 10.7 | 2.7 |
| Completeness [%] | 100.0 | 99.3 |
| Redundancy | 9 | 6.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 1.16 M AMMONIUM PHOSPHATE PH 4.5, SITTING DROP |
