1W1Z
Structure of the plant like 5-Aminolaevulinic Acid Dehydratase from Chlorobium vibrioforme
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-10-01 |
| Detector | ADSC CCD |
| Spacegroup name | P 4 21 2 |
| Unit cell lengths | 125.235, 125.235, 164.603 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.600 |
| R-factor | 0.2905 |
| R-free | 0.38210 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1b4k |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.006 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALED |
| Phasing software | MOLREP |
| Refinement software | SHELX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.740 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.130 | 0.420 |
| Number of reflections | 44567 | |
| <I/σ(I)> | 5.7 | 1.8 |
| Completeness [%] | 99.2 | 97.1 |
| Redundancy | 4.6 | 4.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.5 | pH 8.50 |
