1W14

UROKINASE TYPE PLASMINOGEN ACTIVATOR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	195
Spacegroup name	P 21 21 21
Unit cell lengths	53.460, 54.770, 82.380
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	200.000 - 2.200
R-factor	0.2098
Rwork	0.210
R-free	0.25270
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	1.375
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	200.000
High resolution limit [Å]	2.200
Rmerge	0.130
Number of reflections	11995
Completeness [%]	94.8
Redundancy	2.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1