1VTU
Structural characteristics of enantiomorphic DNA: Crystal analysis of racemates of the D(CGCGCG) duplex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Detector technology | DIFFRACTOMETER |
| Detector | RIGAKU AFC-5 |
| Spacegroup name | P -1 |
| Unit cell lengths | 29.302, 23.215, 23.184 |
| Unit cell angles | 72.96, 90.60, 90.60 |
Refinement procedure
| Resolution | 10.000 - 2.200 |
| R-factor | 0.199 |
| Rwork | 0.199 |
| RMSD bond length | 0.019 |
| RMSD bond angle | 3.760 |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Number of reflections | 2930 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | pH 7.00, VAPOR DIFFUSION, HANGING DROP |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | 2 | 3 |
| 2 | 1 | 1 | MPD | 5 | 6 |
| 3 | 1 | 1 | MGCL2 | 8 | 9 |
| 4 | 1 | 1 | SPERMINE | 11 | 12 |
| 5 | 1 | 1 | NA CACODYLATE | 14 | 15 |
| 6 | 1 | 2 | WATER | 17 | 18 |
| 7 | 1 | 2 | MPD | 20 | 21 |
