1VTN

CO-CRYSTAL STRUCTURE OF THE HNF-3/FORK HEAD DNA-RECOGNITION MOTIF RESEMBLES HISTONE H5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Detector technology	IMAGE PLATE
Detector	RIGAKU RAXIS IIC
Spacegroup name	P 31
Unit cell lengths	74.600, 74.600, 85.050
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	6.000 - 2.500
R-factor	0.211
Rwork	0.211
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.500
Number of reflections	18352

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	5.5		pH 5.50, VAPOR DIFFUSION

Crystallization Reagents

ID	crystal ID	solution ID	reagent name	concentration	details
1	1	1	WATER	2	3
10	1	2	MGCL2	29	30
11	1	2	K ACETATE	32	33
2	1	1	DTT	5	6
3	1	1	KCL	8	9
4	1	1	NH4 ACETATE	11	12
5	1	1	MGCL2	14	15
6	1	1	K ACETATE	17	18
7	1	2	WATER	20	21
8	1	2	DTT	23	24
9	1	2	KCL	26	27