1VT9
The structure and hydration of the A-DNA fragment D(GGGTACCC) at room temperature and low temperature
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SEALED TUBE |
| Detector technology | DIFFRACTOMETER |
| Detector | ENRAF-NONIUS CAD4 |
| Spacegroup name | P 61 |
| Unit cell lengths | 46.800, 46.800, 44.520 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 2.500 |
| R-factor | 0.119 |
| Rwork | 0.119 |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 1582 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 277 | MPD, MgCl2, spermine, sodium cacodylate, temperature 277K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | 2 | 3 |
| 2 | 1 | 1 | MPD | 5 | 6 |
| 3 | 1 | 1 | MGCL2 | 8 | 9 |
| 4 | 1 | 1 | SPERMINE_HCL | 11 | 12 |
| 5 | 1 | 1 | NA CACODYLATE | 14 | 15 |
