1VT5
THE CRYSTAL STRUCTURE OF D(CCCCGGGG): A NEW A-FORM VARIANT WITH AN EXTENDED BACKBONE CONFORMATION
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SEALED TUBE |
| Temperature [K] | 288 |
| Detector technology | DIFFRACTOMETER |
| Detector | NICOLET P3 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 43.360, 43.360, 24.830 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.250 |
| R-factor | 0.24 |
| Rwork | 0.240 |
| Refinement software | CORELS |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.250 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | MPD, Sodium Cacodylate, spermine, MgCl2, pH 7.00 | ||
| 1 | 7 | MPD, Sodium Cacodylate, spermine, MgCl2, pH 7.00 |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | 2 | 3 |
| 2 | 1 | 1 | MPD | 5 | 6 |
| 3 | 1 | 1 | NA CACODYLATE | 8 | 9 |
| 4 | 1 | 1 | SPERMINE | 11 | 12 |
| 5 | 1 | 1 | MGCL2 | 14 | 15 |
| 6 | 1 | 2 | WATER | 17 | 18 |
| 7 | 1 | 2 | MPD | 20 | 21 |
