Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 32-ID |
| Synchrotron site | APS |
| Beamline | 32-ID |
| Temperature [K] | 99.8 |
| Detector technology | CCD |
| Collection date | 2004-06-24 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9792 |
| Spacegroup name | P 1 |
| Unit cell lengths | 51.940, 53.560, 53.480 |
| Unit cell angles | 65.88, 70.37, 70.88 |
Refinement procedure
| Resolution | 25.000 - 2.090 |
| R-factor | 0.21609 |
| Rwork | 0.210 |
| R-free | 0.27655 |
| Structure solution method | SAD |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.474 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.180 |
| High resolution limit [Å] | 2.090 | 2.090 |
| Rmerge | 0.109 | 0.270 |
| Number of reflections | 26115 | |
| <I/σ(I)> | 12.4 | 2.6 |
| Completeness [%] | 92.2 | 73 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 295 | PEG, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 295K |
