1VJH

Crystal structure of gene product of At1g24000 from Arabidopsis thaliana

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 32-ID
Synchrotron site	APS
Beamline	32-ID
Detector technology	CCD
Collection date	2003-12-01
Detector	MARRESEARCH
Wavelength(s)	0.97921
Spacegroup name	P 1 2 1
Unit cell lengths	45.681, 34.261, 78.597
Unit cell angles	90.00, 90.01, 90.00

Refinement procedure

Resolution	21.930 - 2.100
Rwork	0.186
R-free	0.23920
RMSD bond length	0.018
RMSD bond angle	1.513
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	SOLVE (2.02)
Refinement software	REFMAC (refmac_5.1.24)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	30.000	30.000	2.140
High resolution limit [Å]	2.100	5.690	2.100
Rmerge	0.065	0.067	0.100
Number of reflections	14582
Completeness [%]	99.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.5	295	Aceti, D.J., (2003) Biopolymers, 469., Jeon, W.B., (2005) J.Struct.Funct.Genom., 61, 206., Zhao, Q., (2004) J.Struct.Funct.Genom., 5, 87. *