1VGK

The crystal structure of class I Major histocompatibility complex, H-2Kd at 2.0 A resolution

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007
Collection date	2004-01-14
Spacegroup name	P 21 21 2
Unit cell lengths	89.082, 110.389, 47.015
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.060
R-factor	0.1921
Rwork	0.190
R-free	0.24010
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.060
Number of reflections	29503
Completeness [%]	99.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	291	PEG 2000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K