1VDV

Bovine Milk Xanthine Dehydrogenase Y-700 Bound Form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL40B2
Synchrotron site	SPring-8
Beamline	BL40B2
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 4
Wavelength(s)	1
Spacegroup name	C 1 2 1
Unit cell lengths	166.817, 123.940, 148.888
Unit cell angles	90.00, 91.16, 90.00

Refinement procedure

Resolution	20.000 - 1.980
Rwork	0.178
R-free	0.21470
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	EPMR
Refinement software	CNS (1.0)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.980
Number of reflections	186918

Crystallization Conditions

crystal ID	method	pH	temperature	details
1