1V6Y
Crystal Structure Of chimeric Xylanase between Streptomyces Olivaceoviridis E-86 FXYN and Cellulomonas fimi Cex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 292 |
Detector technology | DIFFRACTOMETER |
Collection date | 1999-10-01 |
Detector | WEISSENBERG |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.480, 57.190, 106.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.670 - 2.200 |
R-factor | 0.153 |
Rwork | 0.153 |
R-free | 0.19800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1XYF and 2EXO |
RMSD bond length | 0.005 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.065 | 0.139 |
Number of reflections | 13853 | |
<I/σ(I)> | 17.7 | 10.1 |
Completeness [%] | 88.3 | 77.8 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 294 | ammonium sulfate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |