1V54

Bovine heart cytochrome c oxidase at the fully oxidized state

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Spacegroup name	P 21 21 21
Unit cell lengths	182.590, 205.140, 178.250
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.000 - 1.800
Rwork	0.202
R-free	0.22700
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.012 *
RMSD bond angle	1.870 *
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	200.000 *
High resolution limit [Å]	1.800 *	1.800 *
Rmerge	0.070 *	0.333 *
Total number of observations	3614983 *
Number of reflections	604170 *	59168 *
Completeness [%]	99.2 *	97.8 *
Redundancy	6.0 *	3.9 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *			Yoshikawa, S., (1998) Science, 280, 1723. *