1V2N
Potent factor XA inhibitor in complex with bovine trypsin variant X(99/175/190)bT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 2001-04-12 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 55.240, 55.240, 111.280 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 1.800 |
Rwork | 0.173 |
R-free | 0.19600 |
Structure solution method | FOURIER SYNTHESIS |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 100.000 |
High resolution limit [Å] | 1.800 |
Number of reflections | 18842 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | ammonium sulphate, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |