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1V2J

BENZAMIDINE IN COMPLEX WITH BOVINE TRYPSIN VARIANT X(SSRI)bT.C1

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU300
Temperature [K]287
Detector technologyIMAGE PLATE
Collection date2002-08-02
DetectorRIGAKU RAXIS IV
Spacegroup nameP 21 21 21
Unit cell lengths61.100, 70.340, 64.150
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution10.000 - 1.900
Rwork0.216
R-free0.24100
Structure solution methodFOURIER SYNTHESIS
Data reduction softwareCrystalClear
Data scaling softwareCrystalClear
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 Overall
Low resolution limit [Å]43.880
High resolution limit [Å]1.440
Number of reflections30102
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6295ammonium sulphate, pH 6, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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