1UZL
MabA from Mycobacterium tuberculosis
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-08-15 |
| Detector | MARRESEARCH |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 81.579, 117.159, 52.495 |
| Unit cell angles | 90.00, 122.65, 90.00 |
Refinement procedure
| Resolution | 57.000 - 2.000 |
| R-factor | 0.1873 |
| Rwork | 0.180 |
| R-free | 0.25000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 59.700 | 2.050 |
| High resolution limit [Å] | 1.998 | 1.990 |
| Rmerge | 0.065 | 0.320 |
| Number of reflections | 24747 | |
| <I/σ(I)> | 17.2 | 1.8 |
| Completeness [%] | 99.7 | 99.9 |
| Redundancy | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | PIPES PH 6.6, CSCL 450 MM, PEG 3000 12%, 50MM NADP |
