1URR

A novel Drosophila Melanogaster Acylphosphatase (AcPDro2)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Spacegroup name	P 31 2 1
Unit cell lengths	45.722, 45.722, 98.585
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 1.500
R-factor	0.163
Rwork	0.160
R-free	0.23000
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2acy
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	AMoRE
Refinement software	REFMAC

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.500	1.550
High resolution limit [Å]	1.500	1.500
Rmerge	0.047	0.300
Number of reflections	19859
<I/σ(I)>	17.2	2.9
Completeness [%]	98.7	97.1
Redundancy	6.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		4.5		pH 4.50