1UPD
Oxidized STRUCTURE OF CYTOCHROME C3 FROM DESULFOVIBRIO DESULFURICANS ATCC 27774 AT PH 7.6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 110 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 61.680, 61.680, 106.120 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 1.400 |
R-factor | 0.1472 |
R-free | 0.19120 |
Structure solution method | OTHER |
RMSD bond length | 0.011 |
RMSD bond angle | 0.027 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | SHELX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.430 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.055 | 0.279 |
Number of reflections | 44219 | |
Completeness [%] | 99.2 | 98.5 |
Redundancy | 4.32 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.6 | pH 7.60 |