1UOD

Crystal structure of the dihydroxyacetone kinase from E. coli in complex with dihydroxyacetone-phosphate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Spacegroup name	P 21 21 2
Unit cell lengths	96.498, 97.055, 86.123
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	24.110 - 1.900
R-factor	0.168
Rwork	0.167
R-free	0.20600
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.015
RMSD bond angle	1.718
Refinement software	REFMAC (5.1.19)

Data quality characteristics

	Overall
Low resolution limit [Å]	25.000
High resolution limit [Å]	1.900
Rmerge	0.045
Number of reflections	60809
<I/σ(I)>	31.7
Completeness [%]	94.6
Redundancy	3.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		5		pH 5.00