1UM4
Catalytic Antibody 21H3 with hapten
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-01-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.962, 63.470, 137.549 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.100 - 1.800 |
Rwork | 0.223 |
R-free | 0.24900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.500 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | EPMR |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.100 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 37358 | |
Completeness [%] | 96.0 | 94.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.25 | 277 | PEG4000, lithium sulfate, pH 4.25, VAPOR DIFFUSION, HANGING DROP, temperature 277K |