1ULR

Crystal structure of tt0497 from Thermus thermophilus HB8

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL45XU
Synchrotron site	SPring-8
Beamline	BL45XU
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2003-02-09
Detector	RIGAKU RAXIS V
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	29.911, 45.727, 49.958
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.710 - 1.300
R-factor	0.18958
Rwork	0.187
R-free	0.21632
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2acy
RMSD bond length	0.027
RMSD bond angle	1.858
Data reduction software	CrystalClear ((MSC/RIGAKU))
Data scaling software	CrystalClear ((MSC/RIGAKU))
Phasing software	AMoRE
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	33.730	1.130
High resolution limit [Å]	1.090	1.090
Number of reflections	18506
Completeness [%]	63.7	5.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	micro batch using TERA			micro batch using TERA