1UIE
ANALYSIS OF THE STABILIZATION OF HEN LYSOZYME WITH THE HELIX DIPOLE AND CHARGED SIDE CHAINS
Experimental procedure
| Temperature [K] | 295 |
| Detector technology | IMAGE PLATE |
| Collection date | 1995-02-08 |
| Detector | RIGAKU RAXIS IIC |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 79.440, 79.440, 37.760 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.000 - 1.950 |
| R-factor | 0.17 |
| Rwork | 0.170 |
| Starting model (for MR) | 1rfp |
| RMSD bond length | 0.009 |
| RMSD bond angle | 23.538 * |
| Data reduction software | PROCESS ((SCALE)) |
| Data scaling software | PROCESS ((SCALE)) |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 2.250 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Rmerge | 0.058 | 0.175 |
| Number of reflections | 8629 | |
| Completeness [%] | 93.2 | 87.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 4.7 | 50 MM ACETATE AT PH4.7 CONTAINING 0.9 M NACL |
