1UHJ
Crystal structure of br-aequorin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | OXFORD PX210 |
Wavelength(s) | 0.9 |
Spacegroup name | P 1 |
Unit cell lengths | 34.213, 56.983, 57.820 |
Unit cell angles | 72.22, 80.32, 68.01 |
Refinement procedure
Resolution | 28.190 - 1.800 |
R-factor | 0.16337 |
Rwork | 0.162 |
R-free | 0.19819 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.678 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.500 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 35673 | |
<I/σ(I)> | 13.8 | |
Completeness [%] | 95.4 | 79.9 |
Redundancy | 2 | 1.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.1 | 293 | ammonium sulfate, pH 7.1, VAPOR DIFFUSION, HANGING DROP, temperature 293K |