1UES

Crystal structure of Porphyromonas gingivalis SOD

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL24XU
Synchrotron site	SPring-8
Beamline	BL24XU
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2001-09-28
Detector	RIGAKU RAXIS V
Wavelength(s)	0.836
Spacegroup name	P 21 21 21
Unit cell lengths	71.680, 95.120, 98.750
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 1.600
Rwork	0.221
R-free	0.25000
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	X-PLOR
Refinement software	X-PLOR (98.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.600
Rmerge	0.055
Number of reflections	84510
Completeness [%]	76.0
Redundancy	7.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.8	293	PEG4000, potassium phosphate , pH 5.8, VAPOR DIFFUSION, HANGING DROP, temperature 293K