1UCY

THROMBIN COMPLEXED WITH FIBRINOPEPTIDE A ALPHA (RESIDUES 7-19). THREE COMPLEXES, ONE WITH EPSILON-THROMBIN AND TWO WITH ALPHA-THROMBIN

Experimental procedure

Detector technology	X1000 MULTIWIRE
Detector	SIEMENS
Spacegroup name	P 1 21 1
Unit cell lengths	82.470, 88.780, 98.550
Unit cell angles	90.00, 106.21, 90.00

Refinement procedure

Resolution	7.000 - 2.200
R-factor	0.171
Rwork	0.171
RMSD bond length	0.011
RMSD bond angle	19.400 *
Data reduction software	XENGEN
Data scaling software	XENGEN
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	7.000	2.300
High resolution limit [Å]	2.200	2.200
Rmerge	0.072 *
Total number of observations	117995 *
Number of reflections	45875
Completeness [%]		15

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	8 *		Martin, P.D., (1992) J. Biol. Chem., 267, 7911. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	40 (%)