1U7K
Structure of a hexameric N-terminal domain from murine leukemia virus capsid
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX14.2 |
| Synchrotron site | SRS |
| Beamline | PX14.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-02-01 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9779, 0.970, 0.9783 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 85.995, 78.340, 85.766 |
| Unit cell angles | 90.00, 118.86, 90.00 |
Refinement procedure
| Resolution | 12.000 - 1.850 |
| R-factor | 0.21126 |
| Rwork | 0.210 |
| R-free | 0.24208 |
| Structure solution method | MAD |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.169 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.980 |
| High resolution limit [Å] | 1.850 | 1.900 |
| Rmerge | 0.081 | 0.440 |
| Number of reflections | 85291 | |
| Completeness [%] | 100.0 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
