1TYL

THE STRUCTURE OF A COMPLEX OF HEXAMERIC INSULIN AND 4'-HYDROXYACETANILIDE

Experimental procedure

Spacegroup name	H 3
Unit cell lengths	81.110, 81.110, 37.970
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 * - 1.900
R-factor	0.168
RMSD bond length	0.019
RMSD bond angle	0.047 *
Refinement software	PROFFT

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.900 *	1.900 *
Rmerge	0.034 *
Total number of observations	28940 *
Number of reflections	6783 *
Completeness [%]		46 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	Tylenol	(M)
2	1	1		(M)
3	1	1	sodium citrate	(M)
4	1	1	zinc acetate	(M)
5	1	1	4'-hydroxyacetanilide	(M)
6	1	1	sodium chloride	(M)