1TY8
Crystal structure of yeast ymx7, an ADP-ribose-1''-monophosphatase, complexed with ADP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12C |
| Synchrotron site | NSLS |
| Beamline | X12C |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-10-21 |
| Detector | BRANDEIS - B4 |
| Wavelength(s) | 0.979 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 107.948, 38.054, 63.137 |
| Unit cell angles | 90.00, 111.75, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.100 |
| Rwork | 0.190 |
| R-free | 0.24400 |
| Structure solution method | Difference Fourier |
| Starting model (for MR) | 1njr |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.240 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.180 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.042 | 0.151 |
| Number of reflections | 14060 | |
| <I/σ(I)> | 18 | |
| Completeness [%] | 99.3 | 93.4 |
| Redundancy | 6.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | PEG 6000, Citric acid, NH4Cl, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
