1TXK

Crystal structure of Escherichia coli OpgG

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM30A
Synchrotron site	ESRF
Beamline	BM30A
Temperature [K]	100
Detector technology	CCD
Collection date	2003-07-04
Detector	MARRESEARCH
Wavelength(s)	0.9793, 0.9795, 0.9739
Spacegroup name	P 21 21 21
Unit cell lengths	63.860, 88.120, 215.650
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.990 - 2.500
R-factor	0.192
Rwork	0.192
R-free	0.22900
Structure solution method	MAD
RMSD bond length	0.007
RMSD bond angle	1.400
Data reduction software	XNEMO
Data scaling software	XDS
Phasing software	SHELXD
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.600
High resolution limit [Å]	2.500	2.500
Number of reflections	80513
Completeness [%]	99.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	293	PEG 200, sodium acetate, MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K