1TUD

ALPHA-SPECTRIN SRC HOMOLOGY 3 DOMAIN, CIRCULAR PERMUTANT, CUT AT N47-D48

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1995-06-26
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	31.950, 42.880, 54.190
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 1.770
R-factor	0.184
Rwork	0.184
R-free	0.24800
RMSD bond length	0.009
RMSD bond angle	1.447
Data reduction software	XDS
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	100.000
High resolution limit [Å]	1.770
Rmerge	0.043
Number of reflections	6591
Completeness [%]	90.3
Redundancy	2.64

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *			NMR *