1TRY

STRUCTURE OF INHIBITED TRYPSIN FROM FUSARIUM OXYSPORUM AT 1.55 ANGSTROMS

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	33.300, 67.890, 39.790
Unit cell angles	90.00, 107.33, 90.00

Refinement procedure

Resolution	10.000 - 1.550
R-factor	0.144
RMSD bond length	0.017 *
RMSD bond angle	0.039 *
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	1.550 *
Rmerge	0.051 *
Total number of observations	55012 *
Number of reflections	23178 *
Completeness [%]	94.7 *	69 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	12.5 (mg/ml)
2	1	drop	ammonium sulfate	0.7 (M)
3	1	drop	citrate	50 (mM)
4	1	reservoir	ammonium sulfate	1.4 (M)
5	1	reservoir	sodium citrate	0.1 (M)