1TP9
PRX D (type II) from Populus tremula
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | LURE BEAMLINE DW32 |
| Synchrotron site | LURE |
| Beamline | DW32 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2001-03-03 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.948 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 59.513, 69.112, 76.429 |
| Unit cell angles | 90.00, 93.30, 90.00 |
Refinement procedure
| Resolution | 29.880 - 1.620 |
| R-factor | 0.19266 |
| Rwork | 0.189 |
| R-free | 0.22448 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.804 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.880 | 1.680 |
| High resolution limit [Å] | 1.620 | 1.620 |
| Number of reflections | 79011 | |
| Completeness [%] | 96.1 | 83.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | PEG4000, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
