1TOC
STRUCTURE OF SERINE PROTEINASE
Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1996-01-13 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 125.300, 89.900, 101.400 |
| Unit cell angles | 90.00, 108.40, 90.00 |
Refinement procedure
| Resolution | 10.000 - 3.100 |
| R-factor | 0.23 |
| Rwork | 0.230 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.660 |
| Data reduction software | MOSFLM |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 9999.000 * | |
| High resolution limit [Å] | 3.000 * | 3.000 * |
| Rmerge | 0.140 | |
| Number of reflections | 94484 | |
| Completeness [%] | 89.0 | 75.2 * |
| Redundancy | 2.39 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 5 * | 20 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | PEG4000 | 25 (%) | |
| 2 | 1 | reservoir | ammonium acetate | 160 (mM) | |
| 3 | 1 | reservoir | sodium acetate | 80 (mM) | |
| 4 | 1 | reservoir | ammonium sulfate | 200 (mM) |
