1TLP
CRYSTALLOGRAPHIC STRUCTURAL ANALYSIS OF PHOSPHORAMIDATES AS INHIBITORS AND TRANSITION-STATE ANALOGS OF THERMOLYSIN
Experimental procedure
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 94.100, 94.100, 131.400 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 23.300 - 2.300 |
| R-factor | 0.174 |
| RMSD bond length | 0.022 |
| RMSD bond angle | 2.900 |
| Refinement software | TNT |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 23.300 |
| High resolution limit [Å] | 2.300 |
| Rmerge | NaN * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7.2 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | calcium acetate | 0.01 (M) | |
| 2 | 1 | 1 | Tris acetate | 0.01 (M) | |
| 3 | 1 | 1 | dimethylsulfoxide | 7 (%(v/v)) |
