1TLI
THERMOLYSIN (2% ISOPROPANOL SOAKED CRYSTALS)
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1997-09 |
Detector | MARRESEARCH |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 93.930, 93.930, 130.910 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.050 |
Rwork | 0.165 |
R-free | 0.22700 * |
Structure solution method | ISOMORPHOUS REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.900 * |
Data reduction software | DENZO |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.190 |
High resolution limit [Å] | 2.050 | 2.050 |
Rmerge | 0.112 | 0.346 |
Number of reflections | 20770 | |
<I/σ(I)> | 5.5 | 2.2 |
Completeness [%] | 95.0 | 93 |
Redundancy | 7.2 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.5 | pH 7.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 4.6 (mM) | |
2 | 1 | 1 | DMSO | 45 (%) | |
3 | 1 | 1 | Tris-HCl | 50 (mM) | |
4 | 1 | 1 | 2.5 (M) | pH7.5 |