1TIF

TRANSLATION INITIATION FACTOR 3 N-TERMINAL DOMAIN

Experimental procedure

Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X12C
Synchrotron site	NSLS
Beamline	X12C
Detector technology	IMAGE PLATE AREA DETECTOR
Collection date	1994-04
Detector	MARRESEARCH
Wavelength(s)	0.95
Spacegroup name	P 21 21 21
Unit cell lengths	27.600, 39.200, 65.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.192
Rwork	0.192
R-free	0.23300
RMSD bond length	0.006 *
RMSD bond angle	1.320 *
Data reduction software	MOSFLM
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Rmerge	0.039
Number of reflections	6646
Completeness [%]	95.9
Redundancy	7.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	2.7 (M)
2	1	reservoir	Tris-HCl	0.1 (M)