1TIE

CRYSTAL STRUCTURE OF A KUNITZ-TYPE TRYPSIN INHIBITOR FROM ERYTHRINA CAFFRA SEEDS

Experimental procedure

Spacegroup name	P 65 2 2
Unit cell lengths	73.400, 73.400, 143.000
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 2.500
R-factor	0.208 *
Rwork	0.208
RMSD bond length	0.016
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.065 *
Total number of observations	33533 *
Number of reflections	7770 *
Completeness [%]	93.6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	10 (mg/ml)
2	1	drop	acetate	20 (mM)
3	1	drop		150 (mM)
4	1	reservoir	distilled water