1TGT

ON THE DISORDERED ACTIVATION DOMAIN IN TRYPSINOGEN. CHEMICAL LABELLING AND LOW-TEMPERATURE CRYSTALLOGRAPHY

Experimental procedure

Spacegroup name	P 31 2 1
Unit cell lengths	55.400, 55.400, 108.500
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	6.500 - 1.700
R-factor	0.187 *
Rwork	0.187
RMSD bond length	0.190 *

Data quality characteristics

	Overall
High resolution limit [Å]	1.700 *
Rmerge	0.062 *
Total number of observations	34340 *
Number of reflections	15890 *
Completeness [%]	72.4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	10 (mg/ml)
2	1	drop	pancreatic trypsin inhibitor		at a molar ratio of 4-1
3	1	drop		1.5 (M)
4	1	reservoir		1.5 (M)