1TGS

THREE-DIMENSIONAL STRUCTURE OF THE COMPLEX BETWEEN PANCREATIC SECRETORY INHIBITOR (KAZAL TYPE) AND TRYPSINOGEN AT 1.8 ANGSTROMS RESOLUTION. STRUCTURE SOLUTION, CRYSTALLOGRAPHIC REFINEMENT AND PRELIMINARY STRUCTURAL INTERPRETATION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	67.100, 75.500, 66.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 - 1.800
R-factor	0.195 *
Rwork	0.186

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.084 *
Number of reflections	26341 *
Completeness [%]	84.0 *