1TG0
0.97-A structure of the SH3 domain of bbc1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-01-23 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.91920 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 23.780, 51.320, 28.960 |
| Unit cell angles | 90.00, 102.47, 90.00 |
Refinement procedure
| Resolution | 20.000 - 0.970 |
| Rwork | 0.146 |
| R-free | 0.19310 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1wdx |
| RMSD bond length | 0.014 |
| RMSD bond angle | 0.036 |
| Data scaling software | XDS |
| Phasing software | AMoRE |
| Refinement software | SHELXL |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 28.000 |
| High resolution limit [Å] | 0.970 |
| Number of reflections | 39611 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 295 | 3.2M ammonium sulfate, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 295K |
