1T9P
Crystal Structure of V44A, G45P Cp Rubredoxin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.1 |
| Synchrotron site | ALS |
| Beamline | 8.2.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-08-01 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.0332 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 37.920, 56.450, 38.330 |
| Unit cell angles | 90.00, 112.61, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.500 |
| R-factor | 0.197 |
| Rwork | 0.196 |
| R-free | 0.21500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | CrystalClear |
| Data scaling software | CrystalClear ((MSC/RIGAKU)) |
| Phasing software | AMoRE |
| Refinement software | X-PLOR (3.851) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.550 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Number of reflections | 23325 | |
| Completeness [%] | 97.6 | 97.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
