1T9O
Crystal Structure of V44G Cp Rubredoxin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-08-01 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0332 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 38.450, 57.670, 38.630 |
Unit cell angles | 90.00, 112.85, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.175 |
Rwork | 0.173 |
R-free | 0.18300 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear ((MSC/RIGAKU)) |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 9813 | |
Completeness [%] | 97.4 | 87.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 279 | ammonium sulfate, acetate, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 279K |