1T99
r106g kdo8ps without substrates
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-D |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 84.819, 84.819, 160.262 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.410 - 1.850 |
Rwork | 0.208 |
R-free | 0.24500 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1fx6 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.500 |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | d*TREK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 42.410 |
High resolution limit [Å] | 1.850 |
Number of reflections | 56873 |
<I/σ(I)> | 4.7 |
Completeness [%] | 98.5 |
Redundancy | 10.29 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 277 | PEG 4K, Na-acetate, pH 4.7, VAPOR DIFFUSION, HANGING DROP, temperature 277K |