1T77

Crystal structure of the PH-BEACH domains of human LRBA/BGL

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X4A
Synchrotron site	NSLS
Beamline	X4A
Temperature [K]	100
Detector technology	CCD
Collection date	2003-02-01
Detector	ADSC QUANTUM 4
Wavelength(s)	0.9800
Spacegroup name	P 1 21 1
Unit cell lengths	73.218, 102.239, 131.519
Unit cell angles	90.00, 90.47, 90.00

Refinement procedure

Resolution	20.000 - 2.400
R-factor	0.211
Rwork	0.210
R-free	0.25800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.300
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	COMO
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.480
High resolution limit [Å]	2.400	2.400
Rmerge	0.051
Number of reflections	67350
Completeness [%]	88.9	74

Crystallization Conditions

crystal ID	method	pH	temperature	details
1