1SY1
1.0 A Crystal Structure of T121V Mutant of Nitrophorin 4 Complexed with Nitric Oxide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-02-24 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.751 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 70.395, 42.724, 53.032 |
Unit cell angles | 90.00, 94.31, 90.00 |
Refinement procedure
Resolution | 26.440 - 1.010 |
R-factor | 0.13006 |
Rwork | 0.129 |
R-free | 0.14452 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1koi |
RMSD bond length | 0.013 |
RMSD bond angle | 1.729 |
Data scaling software | d*TREK |
Refinement software | REFMAC (5.1.22) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.600 | 1.040 |
High resolution limit [Å] | 1.010 | 1.010 |
Rmerge | 0.043 | 0.175 |
Number of reflections | 80037 | |
<I/σ(I)> | 16.6 | 6.2 |
Completeness [%] | 96.1 | 88.6 |
Redundancy | 3.66 | 3.46 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | Ammonium Phosphate 3.2 M, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |